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Tables of Contents for Basic Gas Chromatography
Chapter/Section Title
Page #
Page Count
Series Preface
ix
2
Preface
xi
 
1 Introduction
1
13
A Brief History
1
2
Definitions
3
6
Overview: Advantages and Disadvantages
9
3
Instrumentation
12
2
2 Instrument Overview
14
15
Carrier Gas
15
2
Flow Control and Measurement
17
3
Sample Inlets and Sampling Devices
20
4
Columns
24
1
Temperature Zones
25
2
Detectors
27
1
Data Systems
27
2
3 Basic Concepts and Terms
29
26
Definitions, Terms, and Symbols
29
11
The Rate Theory
40
11
A Redefinition of H
51
1
The Achievement of Separation
52
3
4 Stationary Phases
55
18
Selecting a Column
55
1
Classification of Stationary Phases for GLC
56
11
Liquid Stationary Phases (GLC)
67
4
Solid Stationary Phases (GSC)
71
2
5 Packed Columns and Inlets
73
13
Solid Supports
73
2
Liquid Stationary Phases
75
1
Solid Stationary Phases (GSC)
76
3
Gas Analysis
79
3
Inlets for Liquid Samples and Solutions
82
1
Special Columns
83
1
Upgrading for Capillary Columns
84
2
6 Capillary Columns and Inlets
86
15
Types of OT Columns
86
2
OT Column Tubing
88
2
Advantages of OT Columns
90
1
Column Selection
91
6
Capillary Inlet Systems
97
4
7 Detectors
101
25
Classification of Detectors
102
3
Detector Characteristics
105
7
Flame Ionization Detector (FID)
112
4
Thermal Conductivity Detector (TCD)
116
3
Electron Capture Detector (ECD)
119
4
Other Detectors
123
3
8 Qualitative and Quantitative Analysis
126
16
Qualitative Analysis
126
5
Quantitative Analysis
131
11
9 Programmed Temperature
142
11
Temperature Effects
142
2
Advantages and Disadvantages of PTGC
144
2
Requirements of PTGC
146
2
Theory of PTGC
148
2
Special Topics
150
3
10 Special Topics
153
20
GC-MS
153
10
Chiral Analysis by GC
163
1
Special Sampling Methods
164
2
Derivatization
166
7
11 Troubleshooting GC Systems
173
7
Appendixes
180
13
I. List of Symbols and Acronyms
180
3
II. Guidelines for Selecting Capillary Columns
183
2
III. GC: How to Avoid Problems
185
2
IV. Calculation of Split Ratio for Split Injection on OT Columns
187
1
V. Operating Conditions for Capillary Columns
187
1
VI. OV Liquid Phases Physical Property Data
188
2
VII. Some Pressure Correction Factors (j)
190
1
VIII. List of Some Chromatographic Supply Houses
191
1
IX. Other Resources
192
1
Index of Applications
193
1
Index
194