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Tables of Contents for The Essence of Chromatography
Chapter/Section Title
Page #
Page Count
Preface
ix
General Concepts in Column Chromatography
1
78
Introduction
2
1
Family Tree of Chromatographic Methods
2
4
Zone Migration
6
2
Retention
8
16
Band Broadening
24
27
Resolution
51
8
Separation Time
59
3
Principles of Quantification
62
10
References
72
7
The Column in Gas Chromatography
79
83
Introduction
80
3
Mobile Phases
83
3
Stationary Phases
86
34
Retention in Gas-Liquid Chromatography
120
22
Preparation and Evaluation of Open Tubular Columns
142
14
Preparation and Evaluation of Packed Columns
156
6
References
162
105
Instrumental Aspects of Gas Chromatography
171
1
Introduction
172
1
Pneumatic Systems
172
4
Thermal Zones
176
1
Sample Handling Devices
177
3
Sample Inlets
180
23
Supercritical Fluid Inlets
203
1
Vapor Sample Inlets
204
12
Coupled-Column Gas Chromatography
216
8
Column Connectors and Flow Splitters
224
1
Detectors
225
32
References
257
10
The Column in Liquid Chromatography
267
164
Introduction
269
1
Column Packing Materials
270
30
Retention Mechanisms
300
62
Method Development
362
31
Column Preparation
393
20
References
413
18
Instrumental Aspects of Liquid Chromatography
431
68
Introduction
432
2
Solvent Delivery Systems
434
7
Sample Inlets
441
8
Guard and Scavenger Columns
449
1
Column Temperature Control
449
2
Coupled-Column Systems
451
4
Detectors
455
32
Postcolumn Reaction Systems
487
3
Indirect Detection
490
1
References
491
8
Thin-Layer Chromatography
499
70
Introduction
500
1
Attributes of Layers and Columns
501
3
Theoretical Considerations
504
16
Stationary Phases
520
7
Sample Application
527
2
Multimodal (Coupled Column-Layer) Systems
529
2
Development Techniques
531
10
Method Development
541
11
Detection
552
10
References
562
7
Supercritical Fluid Chromatography
569
50
Introduction
570
3
Mobile Phases
573
7
Stationary Phases
580
2
Kinetic Optimization
582
5
Retention
587
9
Instrumental Aspects
596
12
Related Techniques
608
3
References
611
8
Capillary-Electromigration Separation Techniques
619
100
Introduction
620
3
Capillary Electrophoresis
623
21
Micellar Electrokinetic Chromatography
644
15
Capillary Electrochromatography
659
9
Capillary Gel Electrophoresis
668
3
Capillary Isoelectric Focusing
671
2
Capillary Isotachophoresis
673
3
Method Development
676
8
Instrumental Aspects
684
22
References
706
13
Spectroscopic Detectors for Identification and Quantification
719
74
Introduction
720
1
Mass Spectrometry
721
46
Fourier Transform Infrared Spectrometry
767
12
Nuclear Magnetic Resonance Spectroscopy
779
6
References
785
8
Separation of Stereoisomers
793
54
Introduction
794
3
Enantioselectivity and Absolute Configuration
797
3
Separation of Enantiomers
800
2
Chiral Stationary Phases
802
19
Chiral Mobile Phase Additives
821
9
Complexation Chromatography
830
4
Separation of Enantiomers as Covalent Diastereomer Derivatives
834
3
Liquid-Crystalline Stationary Phases
837
2
References
839
8
Laboratory-Scale Preparative Chromatography
847
54
Introduction
848
1
Thin-Layer Chromatography
848
2
Column Liquid Chromatography
850
34
Supercritical Fluid Chromatography
884
2
Gas Chromatography
886
3
Countercurrent Chromatography
889
4
References
893
8
Subject Index
901